Could one say "i will never see these again" referring to a person's eyes? Or would "i will never see those again" sound better? "i will never see them again"?🤔 it's for a song :)

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I’ll never see them again probably will work better.

I think the grammar allows for either one but them again sounds more natural. “Those” and “These” are going to be used when you repeat the noun: those eyes, these eyes. “Them eyes” is no good. Otherwise I can’t think of a good rule for you.

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I'll never see them again

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I understood what you ment after reading last sentence, so "I will never see them again" is correct. Those and these is used with nouns. For example: I will never see these eyes again.